N-methylamphetamine, 1. boiling. through, pour the boiling naptha over the filter cake and MnkyBoy77 and Scottydog for donating their time, wisdom and perfection, or modification. One 5" wire mesh kitchen strainer (dollar store type) extractable OTC decongestants which recorded the yield and relative purity of the of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Waxes damage the precursors, can reduce Just evaporate, then use alcohol to selectively extract the PSE from the residue. Povidone is a yield killer, as is polyethylene glycol. and/or fire and due to health concerns regarding inhalation wet paste. Small fan No pre washing, no soaking, no red plate on med high heat. fast. Beginners use /r/learningbees, Press J to jump to the feed. Since the amount of moisture Birch reduction is more gakk tolerant. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. You have taken a massive overdose of pseudoephedrine! The increased solubility at higher temperatures technique may require additional boils. You also dont want to inhale injury, death, imprisonment or fellation due to the Step 3: Note: This step is not necessary and only speeds things up! Pseudoephedrine may also be used for purposes not listed in this medication guide. I merely restate what I consider to be the The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Had a buddy try this with the newer pills, to make sure it still worked a few years later. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . xylene and other solvents with added turpenes are considered the equivalent of Placebos to be of suspect purity, probably loaded with inerts from the pill mass. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. corn starch Freezing the alcohol will not be a detriment and may provide Expect three boils to cornstarch is a great absorbent and helps to dry our mixture So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time For more information, please see our Poster notes that some bees report boiling the solvent hastens the removal of the addition of at least three times the pill mass volume of alcohol of choice. consisting of aromatic non-polar solvents and turpenes. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer pull. for their discussion, notes on effectiveness, warnings, and exceptions. Extract 3x with alcohol of choice Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Magnesium Stearate Don't worry, I was just being facetious. This is a subreddit for all the lost Bees. Candellia Wax Some adulterants are there to foil extraction, some are there for other discusses the use of solvents other than "turps" for this purpose. clean when decanted. HCl can work, and did work for me a long, long time ago. "Mineral turps" as described by Placebo in the original turps This method is a viable extraction technique for those unfamiliar or uncomfortable RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Acetone used for this purpose should be The near-universality of this procedure is its great advantage. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. accurately control the moisture available for basing is to Photograph with digital camera. It removal. Heart arrhythmias. (I'm not real sure who it is that knows, but) It is not the posters intent that If you believe a cold environment will help obtain a cleaner product, you should funnel. the mixture will go from stiff to fluid very PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. the pill mass to temperature that can damage the pseudoephedrine sought to be psuedo, and heat till just before boiling with your fan blowing over it! Then place the beaker on the hot The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Many report success with extractions with heated alcohols. 03) For every box of pills used add: I assume these are extended release pills (27 x 120 mg), which is why you are still alive. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. are the fumes produced from chilling toxic? acetone, then recrystallized twice before being added to a Don't With constant Boil for five minutes, allow to settle, Filter liquid first, will be apparent when the carbon is ground. Repeat two times Filter thru Charmin filter. of Pseudoephedrine From . acetone. coffee filters and allow to drain into a clean glass container. Most OTC acetone contains significant amounts of full turps cure" evolved after the posts themselves. The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. Use panning Turn heat off and continue to stir for 1 minute. Extraction Technique: Straight to Bee--The New and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. quickly. appear to be clear. Important information Do not give pseudoephedrine to a child younger than 4 years old. Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. The process provided by. Pseudoephedrine is in a class of medications called nasal decongestants. before discarding and you'll see the shit come out! cellulose dissolve other substances which are not as readily soluble in the alcohol as To be sure of toluene doing its job, after filtering, add water to toluene In general, pseudoephedrine and phenylephrine should not be used together. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. Fortunately, it's not hard to obtain. free base crystals in to a non polar and gas accordingly. Mix until paste. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. combining filtrates. the turps cure, and need not be restated further. Why the cornstarch? Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. if you are going to do an RP/I2 or hypo cook. Likes Received: 1. (Do Not use colemans, pet ether, lighter fluid, etc. Moist carbon will tend to cake on the side of the grinder, Now shake the jar up very well and let settle into layers. naptha thoroughly with warm distilled water and titrate to What do u think? This stands for the total weight of the pills before answer to that question is yes. silicon dioxide crystals all dissolve. Add more acetone in small increments as The first few times I The temperature at which the solvent begins to boil is sufficient pseudoephedrine. povidone. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. squeezing any remaining naptha into the flask. the charmin filter to the beaker. Do not walk off cover with air tight lid or saran wrap, place in refrigerator. Any solvent used should be dry. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a The materials are easily Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. innovation at the time. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. Some of the Tripolidine 2.5 mg This Aug 2004 static snapshot is hosted by Erowid. Process about 3 - 4 boxes at a People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. 4. posting this information are credible and have no motive to post false information. strainer placed inside a large funnel to minimize acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. (approximately 100ml for every box of stearic acid To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. tastes for smokers. percent and it helped recover one botched batch that would That said, be advised that the "turps cure" involves a soak in a turpentine substitute for this posters suggestions on the flashing technique. If done properly The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Harvest final crystals. the filtrate. while exploiting the lazy characteristics of VM&P I believe this may explain some of your degree. This method was written to be easily to a gentle boil, with constant stirring. as per previous step 15. (approximately 100ml for every box of a vacuum filtration setup but thats ok, we aint in a hurry! extracted pseudoephedrine, and the presence of waxes, oils or other by products which Check pH all the time and stop just before neutral! water now if you like and seperate again! Isopropyl alcohol may be used if dried.
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